Local hope and reigning champion Bianca Andreescu blew an early lead as she was toppled by Ons Jabeur in the Round of 16 at the National Bank Open in Montreal.
Tunisian 13th seed Jabeur defeated the Canadian second seed 6-7 (5-7) 6-4 6-1 in two hours and 39 minutes on Thursday.
The come-from-behind triumph was the second time in two matches that the Tunisian has rallied from a set down to win after beating Daria Kasatkina in three.
Jabeur had twice been a break up in the opening set before Andreescu claimed it in an tiebreak.
The 26-year-old Tunisian, who made the Wimbledon quarter-finals this year, responded by breaking at 5-4 to win the second set.
After Andreescu had an injury scare after landing awkwardly on her left foot late in the second set, Jabeur dominated the third, finishing by winning eight of the final nine games.
Jabeur finished with 9-3 aces and was more effective on serve, going at an 81.6 win percentage on her first serve (40 from 49 points).
The lower side of the draw has opened up for the Tunisian who will face Jessica Pegula in the quarter-finals after the unseeded American defeated countrywoman Danielle Collins 6-4 3-6 7-5.
Two-time Wimbledon champion and seventh seed Petra Kvitova was knocked out in a shock by Italian Camila Giorgi in straight sets.
Giorgi, ranked 71st in the world, won 6-4 6-4 in one hour and 36 minutes and will face Cori Gauff in the quarter-finals after she had another walkover against Johanna Konta.
Top seed Aryna Sabalenka had no such problems, cruising past Canadian Rebecca Marino 6-1 6-3 inside an hour.
Sabalenka sets up a quarter-final clash with fellow Belarussian and two-time Australian Open winner Victoria Azarenka.
Azarenka got past Greek 11th seed Maria Sakkari in three sets, 6-4 3-6 7-6 (7-2).
Fourth seed Karolina Pliskova got past Amanda Anisimova 6-1 7-6 (10-8) and will play Sara Sorribes Tormo in the last eight after she won in three sets over Katerina Siniakova.
World number one Swiatek sees off Xiyu in Madrid opener
World number one Iga Swiatek overcame Wang Xiyu with the minimum of fuss on Thursday to progress to the third round of the Madrid Open.
Swiatek has yet to win the title in Madrid, which is the only clay-court European event at which the Pole has not triumphed, but she got off to a flying start with a 6-1 6-4 victory over Xiyu.
"I love this place. I got to know the city a little better last year," Swiatek said. "So this time I feel more comfortable around."
Next up for the 22-year-old is a third-round tie against 27th seed Sorana Cirstea on Saturday.
Data Debrief
Swiatek has registered 150 match wins on the WTA Tour since the start of 2022. Elena Rybakina and Coco Gauff are the next best with 108 wins each.
She also became the first player born this century to claim 50 combined match wins in Madrid, Rome and Roland-Garros, since the inaugural women's singles event at the Madrid Open in 2009.
Dominant Gauff double bagels Rus at Madrid Open
Coco Gauff made a flying start to her Madrid Open campaign on Thursday, recording the first double bagel main-draw win of her career as she cruised past Arantxa Rus to reach the round of 32.
Gauff needed just 51 minutes to see off 33-year-old Rus as she booked a meeting with Ukraine's Dayana Yamstremska for Saturday.
The US Open champion lost just 18 points throughout the match – eight in the opener and 10 in the second set – as she put any doubts over her recent form to bed in emphatic fashion.
Gauff's power proved too much for Rus in the opener, the third seed winning 88 per cent of points behind her first serve and converting three of four break points to go a set up in just 23 minutes.
Rus brought up four break points midway through the second set, but when she failed to convert them, Gauff punished her in ruthless fashion by reeling off another three games then finishing things with a terrific forehand winner.
Speaking after her win, the American said: "I played really well today. It was just one of those days for me… 6-0 6-0, I've never done that before, I'll probably never do it again."
Data Debrief: Gauff matches Azarenka, Halep feat
Gauff is just the third player to register a 6-0 6-0 win in the women's singles draw at the Madrid Open, following in the footsteps of two former world number ones in Victoria Azarenka and Simona Halep.
The American, who only turned 20 last month, is also the youngest player to double bagel an opponent in any main-draw match on the WTA Tour since Iga Swiatek did so against Karolina Pliskova in the 2021 Italian Open final in Rome.
Nadal cruises past teen Blanch to tee up De Minaur rematch in Madrid
Darwin Blanch presented little challenge for Rafael Nadal, who dropped just one game in a convincing 6-1 6-0 triumph at the Madrid Open.
Nadal is feeling his way back to fitness, but 16-year-old qualifier Blanch offered little resistance to the 22-time major champion on Thursday.
Making his farewell appearance at the Madrid Open, where he has won five titles, Nadal needed just 64 minutes to progress to round two.
"I think today I played against an opponent with a great future in front [of him], but today, still making mistakes," said Nadal.
"I just tried to be there, be solid all the time without taking a lot of risks. It worked well. I'm happy to be through and I wish him all the very best for the future."
Nadal's reward is a rematch with Alex de Minaur, who he lost to last week in Barcelona.
Data Debrief
This game saw the largest age gap (21 years, 117 days) between two opponents in the history of ATP Masters 1000 events.
Nadal has now registered 57 wins at the Madrid Open, which is 20 clear of any other player.
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