Cameron Norrie suffered an agonising end to his Australian Open run as he was pipped in a fifth-set tie-break by Alexander Zverev after a terrific fourth-round tussle.
The British number one broke new ground with a brilliant attacking display to defeat Casper Ruud on Saturday and again showed the new dimensions he has added to his game to push the sixth seed all the way.
Norrie, who had not won a set in their four previous meetings, twice came from behind to force a decider but it is Zverev who moves through to the quarter-finals after a 7-5 3-6 6-3 4-6 7-6 (10/3) victory.
Norrie will leave Australia, though, knowing that he can mix it with the best players in the world on the biggest stage and with confidence fully restored after a shaky second half of last season.
The match was briefly interrupted in the third set by a protester, who threw ‘Free Palestine’ flyers onto the court from the front row of Margaret Court Arena before being forcibly escorted away by two spectators.
The scenes were reminiscent of Wimbledon last summer, when Just Stop Oil protesters threw jigsaw pieces and confetti onto the court during two matches, although the leaflets were swiftly cleared here and play quickly resumed.
Norrie’s tactics against Ruud came as no surprise to Zverev, who spent the off-season practising with the British number one in Monte-Carlo.
There were few rallies of any kind in the first set, with serve dominating until Norrie, who was trying to beat a top-10 opponent at a slam for the first time, was broken at 5-5.
Zverev immediately came under pressure on serve for the first time but saved a break point with a forehand onto the line, and looked to have taken control of the contest when he broke again to lead 3-2 in the second.
However, Norrie played what must be one of the best returning games of his career to hit straight back, finishing it off with a zinging backhand cross-court winner.
And Norrie was not finished there, the 28-year-old showing his new-found aggression and willingness to mix up his tactics to pile more pressure on Zverev in his next service game.
The German saved two break points but then mis-hit a forehand on the third and suddenly Norrie was serving for the set.
It was far from straightforward for the 19th seed but he saved four break points before taking it, fortuitously, when a forehand hit the top of the net and dropped over.
A poor service game at 1-2 in the third set was enough for Zverev to take it and though Norrie pushed hard at the beginning of the fourth set, Zverev managed to save two break points in the second game.
However, the Olympic champion was powerless to stop Norrie forcing a decider, the 28-year-old creating two set points at 4-5 and taking the first with a delicate half-volley.
Norrie was managing to bully Zverev, one of the most powerful players on tour, at times from the baseline, while his drop shots and short angled slices kept the German guessing.
They exchanged breaks of serve at the start of the fifth set while Norrie survived a tense game at 3-3, saving three more break points.
Both men managed to hold serve through to a first-to-10-points tie-break but there Norrie’s resistance ran out, with Zverev clinching the win after four hours and five minutes to end British interest in the singles.
Auger-Aliassime and Shapovalov sweep aside Finland at Davis Cup
Felix Auger-Aliassime and Denis Shapovalov moved Canada to the brink of qualification in the Davis Cup Finals group stage, comfortably dispatching Finland in Manchester.
Shapovalov needed just an hour and 13 minutes to beat Eero Vasa 7-6 (7-2) 6-2, backing up his win against Argentine Francisco Cerundolo on Tuesday.
The Canadian served five aces to his opponents' three, producing three love games in the final set to get his nation off to a flying start.
Auger-Aliassime followed up Shapovalov's victory with another straight sets win, this time over Otto Virtanen, emerging a 6-2 6-3 victor.
The world number 21 was dominant on serve throughout his 73-minute triumph, saving all three break points he faced and winning 86% of his first-serve points.
Auger-Aliassime and Shapovalov then prevailed in the doubles against Harri Heliovaara and Virtanen in another straight sets win, putting them top of Group D without dropping a set against their opponents.
Nadal confirms Laver Cup withdrawal to help Team Europe 'deliver the win'
Rafael Nadal confirmed he will not participate in next month's Laver Cup, believing there are "other players who can help the team deliver the win" for Team Europe.
Nadal last played at the Paris Olympics alongside Carlos Alcaraz in the men's doubles, with the Spanish duo knocked out at the quarter-final stage at Roland Garros.
The 38-year-old also competed in the singles but was hampered by a thigh problem in Paris and suffered a second-round loss to eventual gold medallist Novak Djokovic.
Nadal participated in the inaugural edition of the Laver Cup seven years ago, defeating Jack Sock to help Team Europe claim a 15-9 victory.
It is yet to be confirmed who will replace the 22-time grand slam champion in Berlin next month as captain Bjorn Borg now goes in search of adding to his star-studded line-up.
Alexander Zverev, Alcaraz, Daniil Medvedev, Casper Ruud and Stefanos Tsitsipas have already been confirmed as the participants to face Team World in Berlin.
Nadal posted a statement on social media, saying that he was making the decision for the benefit of the team.
“I’m really disappointed to share that I won’t be able to compete at the Laver Cup in Berlin next week," Nadal said.
"This is a team competition and to really support Team Europe, I need to do what’s best for them and at this moment there are other players who can help the team deliver the win.
"I have so many great, emotional memories from playing in the Laver Cup, and I was really looking forward to being with my teammates and with Bjorn in his final year as Captain.
"I wish Team Europe the very best of luck and will be cheering them on from afar.”
The news will accelerate speculation that retirement could be imminent for the Spaniard, who was unsure of his future following his exit from the Olympic Games.
Alcaraz grinds through to help Spain to Davis Cup win
Carlos Alcaraz got a stroke of luck as he helped Spain make a winning start to the Davis Cup Finals group-stage campaign against Czechia as Tomas Machac retired through injury.
The French Open and Wimbledon champion dropped the first set 6-7 (3-7), but rallied to finish the second 6-1, forcing a decider after getting two vital breaks.
However, Machac pulled up in the opening game of the third set with cramp and was unable to carry on after one hour and 41 minutes on the court.
It followed Roberto Bautista's flying start in their opening singles match in Group B as he cruised past Jiri Lehecka 7-6 (7-1) 6-4, with the Czech making 27 unforced errors as he failed to find an edge.
In the doubles, Alcaraz and Marcel Granollers then had to dig deep, coming from behind to beat Adam Pavlasek and Jakub Mensik in three sets to give Spain a 3-0 victory and take them top of the group.
Meanwhile, Great Britain also made a bright start to their campaign in Group D, despite US Open semi-finalist Jack Draper sitting out.
Dan Evans got them started in Manchester with a hard-earned 7-6 (7-3) 6-2 victory over Eero Vasa of Finland, converting both of his break points in the second set.
Billy Harris followed that up with an impressive tournament debut, looking unflappable as he earned the hosts an unattainable lead with his 6-4 7-6 (7-4) win over Otto Virtanen.
Finland got themselves on the board in the doubles though, with Evans and Neal Skupski unable to get the better of Harri Heliovaara and Virtanen ensuring it was only a 2-1 loss.
Elsewhere, the United States joined Germany at the top of Group C with their 3-0 win over Chile and Italy's Matteo Arnaldi held off a spirited Thiago Monteiro to put them in control against Brazil in Group A after Matteo Berrettini's earlier victory.
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