Iga Swiatek’s reign as US Open champion, and world number one, was ended by her nemesis Jelena Ostapenko.
The 22-year-old Pole had not dropped a set on her way to the fourth round, but she had never beaten Ostapenko in three previous career meetings.
Swiatek took the first set with relative ease but then Ostapenko’s sledgehammer of a forehand started finding its mark to level the match.
A one-sided final set saw former French Open champion Ostapenko triumph 3-6 6-3 6-1.
Swiatek’s defeat means that Aryna Sabalenka of Belarus will take over as world number one after the tournament.
Ostapenko will face Coco Gauff in the quarter-finals after the teenager ended the grand slam comeback of mother-of-two Caroline Wozniacki.
The 19-year-old came from a break down in the first and third sets to win both and complete a 6-3 3-6 6-1 victory.
Wozniacki’s return has been one of the stories of New York this year, having come out of retirement after more than three years and two children later.
The 33-year-old former world number one has looked as though she has never been away, but a fired-up Gauff proved just too strong in the deciding set.
Wozniacki got off to a dream start with a break in the first game and a 2-0 lead.
But Gauff quickly got back on the board, levelling at 3-3 before going on to clinch the first set without dropping another game.
Wozniacki cranked up the pressure in the second and Gauff started feeling it as her suspect forehand began to misfire and she was broken for 5-3 as the Dane levelled the match.
Gauff looked uncomfortable as she dropped serve again at the start of the decider, but after pointedly ignoring the advice of coach Brad Gilbert, the wound-up American began firing backhand winners as if they were going out of fashion.
She reeled off the next six games to clinch the victory and let out a loud scream of triumph after converting match point.
“Definitely getting it to 2-1 (in the third set) was the turning point,” said Gauff.
“I got broke and I showed I was still in the match. I started to go for my shots.
“Caroline, it’s like she’s never left, the level she played was amazing. It’s weird because I grew up watching Caroline and when she won the Australian Open, so to be on court with her today was an honour.
“She definitely gets to a lot of balls. I felt a bit like I was playing myself. I knew I had to play aggressive and go for my shots. In some moments I miss but I was happy I could get back and refocus.”
It will be the fifth grand slam quarter-final of Gauff’s still-fledgling career and her second at Flushing Meadows.
“I’ve been in this position before,” she added. “And I think I have confidence in myself that I can go even further.”
'I cannot thank you enough' - Nadal salutes supporters after Madrid Open farewell
Rafael Nadal paid tribute to supporters after his farewell appearance at the Madrid Open ended following defeat to Jiri Lehecka in the last 16.
The 22-time grand slam champion bowed out after going down in straight sets against his Czech opponent, who prevailed 7-5 6-4 to set up a quarter-final clash with Daniil Medvedev.
Nadal was honoured following the conclusion of the final match at his home ATP Masters event, where he triumphed in 2008, 2010, 2013, 2014 and 2017.
Five banners to represent each of his titles were unfurled, displaying the message 'Gracias Rafa', while he was also presented with a trophy by tournament CEO Gerard Tsobanian and director Feliciano Lopez.
"It's been a very special week for me, very positive in many ways, both personally and for my tennis," he said during his on-court interview.
"I had the chance to play again on court. A few weeks ago, two days before Barcelona, I didn’t know if I would compete in an official match again, and I've now played two weeks. It's been unforgettable.
"This is one of those days that when it arrives, it's very tough, but life and my body have been sending me signals for a long time.
"The only thing I can say is thank you. It's been an incredible journey that started when I was little. I came to Madrid for the first time in 2003, when the tournament was played indoors.
"The first time I came here feeling competitive was in 2005. It was one of the most exciting wins of my career. Ever since, the support has been unconditional from everyone. I cannot thank you enough.
"Even though it's not over, this is the last time I'll be in Madrid. You have given me a gift for the last 21 years that's more significant than any Grand Slam I have won. The emotions of playing in Madrid, in front of the Spanish fans, is something that will stay with me forever."
Swiatek admits she would swap shirts with 'huge inspiration' Nadal
Iga Swiatek admits that, like Pedro Cachin, she would also swap shirts with Rafael Nadal following his Madrid Open exit.
The 22-time grand slam champion's farewell appearance at the clay-court ATP Masters tournament, which he has won five times, was ended by a straight-sets defeat to Jiri Lehecka.
Nadal had beaten Cachin in the last 32, with the Argentine subsequently asking his idol for his shirt as a memento following their clash.
Although Swiatek has never been tempted to follow suit with an opponent, the world number one acknowledged she might make an exception for the Spaniard.
"If I would play against Rafa, for sure I would ask for a T-shirt," she laughed.
"For sure, he was a huge inspiration. When I was younger, he was basically the only player I looked up to, but not because of his game on clay - more because of the way he is off the court and how he never gives up, and also his mentality."
Swiatek is through to the semi-finals in the ladies' draw after recovering from losing the opening set to defeat Beatriz Haddad Maia 4-6 6-0 6-2.
The Pole, who will play former US Open runner-up Madison Keys in the last four, equalled Serena Williams and Maria Sharapova as the fastest player to reach 25 WTA 1000 wins on clay, doing so in just 29 matches.
Nadal slumps out of Madrid Open as farewell appearance comes to a halt
Jiri Lehecka claimed a memorable win over one of tennis' greats as he downed Rafael Nadal at the Madrid Open.
Nadal's farewell appearance at the tournament he has won five times came to an end with a 7-5 6-4 defeat on Tuesday.
The 22-time grand slam champion had been hoping to tee up a quarter-final against Daniil Medvedev.
Ultimately, though, world number 31 Lehecka was the man who progressed.
Lehecka ruined the hopes of the Nadal fans packed into the stands in the Spanish capital, and took control when he reeled off 10 straight points to take the opening set.
Nadal won the Madrid Open in 2008, 2010, 2013, 2014 and 2017, and said farewell to the crowd in an on-court interview following his defeat.
Data Debrief: Nadal falls short of milestone
Nadal had been hoping to win his 60th match at the Madrid Open, while he would have reached his 100th ATP Masters 1000 quarter-final had he won. This was his first defeat to a player ranked lower than 20th in the world since he went down to Pablo Cuevas in 2016.
Lehecka, meanwhile, will make his second appearance in the last eight of a Masters 1000 event.
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