Katie Boulter stunned last year's Wimbledon runner-up Karolina Pliskova at the Eastbourne International as the Briton secured the first top-10 scalp of her career.
Despite making a strong start, fourth seed Pliskova faltered and lost 1-6 6-4 6-4 to the world number 127 in the pair's last-32 match.
Boulter said: "I'm super-proud of myself today. I went out there and didn't feel great on court, and I worked so hard to battle and fight, and against a player like that it means so much to me, coming through that."
There was another major shock win for a British player later in the day as Jodie Burrage knocked out top seed Paula Badosa, the world number 169 triumphing 6-4 6-3 against a player who will be seeded fourth at Wimbledon.
Defending champion Jelena Ostapenko beat Ajla Tomljanovic 6-4 6-4 and two-time Wimbledon winner Petra Kvitova saw off Donna Vekic 6-1 7-6 (7-1), while Beatriz Haddad Maia's strong form on grass continued with a 6-4 3-6 6-3 victory over Estonian veteran Kaia Kanepi.
Brazilian left-hander Haddad Maia is coming off the back of title wins in Nottingham and Birmingham and stretched her winning run on grass to 11 matches.
There were also wins in Eastbourne for Camila Giorgi, Madison Keys and Barbora Krejcikova, but Greek third seed Maria Sakkari bowed out, losing 3-6 7-5 6-4 to Ukrainian Anhelina Kalinina.
At the Bad Homburg Open in Germany, the 2019 Wimbledon champion Simona Halep scrambled for a 4-6 6-3 6-4 win against Katerina Siniakova, and sixth seed Amanda Anisimova came from a set down to see off Alison van Uytvanck in a third-set tie-break.
Bianca Andreescu saw off Martina Trevisan 6-3 6-1 and Angelique Kerber also won in straight sets, while top seed and recent French Open semi-finalist Daria Kasatkina reached the quarter-finals with a 6-1 3-6 6-1 win over Germany's Jule Niemeier.
Kasatkina will be absent from Wimbledon due to the ban on Russian players.
Rybakina continues clay winning streak with victory over Bronzetti
In-form Elena Rybakina has moved into the last 32 of the Madrid Open after a straight sets victory over Italian Lucia Bronzetti.
Number four seed Rybakina triumphed 6-4 6-3 on Friday and will next face either Marta Kostyuk or Mayar Sherif.
Rybakina was broken early in each set but ultimately had few problems getting over the line, converting four of her five break points to continue an impressive run of results after winning the Stuttgart Open last week.
She has now won five consecutive WTA matches and has 13 straight wins on clay courts to her name in a superb streak that started one year ago.
Data Debrief: Rybakina in elite company
Since the start of 2020, only two other players have claimed as many 13 consecutive WTA wins on clay, and they are Iga Swiatek and Simona Halep, so Rybakina is in elite company.
Rybakina's last defeat on this surface came in the 2023 edition of the Madrid Open, when she fell to Anna Kalinskaya in her first match, so this win represented a better start to her campaign in the Spanish capital.
World number one Swiatek sees off Xiyu in Madrid opener
World number one Iga Swiatek overcame Wang Xiyu with the minimum of fuss on Thursday to progress to the third round of the Madrid Open.
Swiatek has yet to win the title in Madrid, which is the only clay-court European event at which the Pole has not triumphed, but she got off to a flying start with a 6-1 6-4 victory over Xiyu.
"I love this place. I got to know the city a little better last year," Swiatek said. "So this time I feel more comfortable around."
Next up for the 22-year-old is a third-round tie against 27th seed Sorana Cirstea on Saturday.
Data Debrief
Swiatek has registered 150 match wins on the WTA Tour since the start of 2022. Elena Rybakina and Coco Gauff are the next best with 108 wins each.
She also became the first player born this century to claim 50 combined match wins in Madrid, Rome and Roland-Garros, since the inaugural women's singles event at the Madrid Open in 2009.
Dominant Gauff double bagels Rus at Madrid Open
Coco Gauff made a flying start to her Madrid Open campaign on Thursday, recording the first double bagel main-draw win of her career as she cruised past Arantxa Rus to reach the round of 32.
Gauff needed just 51 minutes to see off 33-year-old Rus as she booked a meeting with Ukraine's Dayana Yamstremska for Saturday.
The US Open champion lost just 18 points throughout the match – eight in the opener and 10 in the second set – as she put any doubts over her recent form to bed in emphatic fashion.
Gauff's power proved too much for Rus in the opener, the third seed winning 88 per cent of points behind her first serve and converting three of four break points to go a set up in just 23 minutes.
Rus brought up four break points midway through the second set, but when she failed to convert them, Gauff punished her in ruthless fashion by reeling off another three games then finishing things with a terrific forehand winner.
Speaking after her win, the American said: "I played really well today. It was just one of those days for me… 6-0 6-0, I've never done that before, I'll probably never do it again."
Data Debrief: Gauff matches Azarenka, Halep feat
Gauff is just the third player to register a 6-0 6-0 win in the women's singles draw at the Madrid Open, following in the footsteps of two former world number ones in Victoria Azarenka and Simona Halep.
The American, who only turned 20 last month, is also the youngest player to double bagel an opponent in any main-draw match on the WTA Tour since Iga Swiatek did so against Karolina Pliskova in the 2021 Italian Open final in Rome.
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